ECC-Opto-10

Test cell for optical characterization in the reflective mode.

Request a quote Data sheet (PDF)Videos

ECC-Opto-10

Test cell for optical characterization in the reflective mode.

Product overview
Videos
Data sheet (PDF)
Request a quote

Product overview

Product description

The ECC-Opto-10 test cell is an advanced next generation battery test cell. It is designed for operando characterization of electrodes using light microscopy, Raman spectroscopy or XRD in reflection mode.
A newly developed sealing concept utilizing laser-welded glass-to-metal electrode feedthroughs and foil seals substantially increases cycle stability compared to the previous generation. The much more compact and low profile design allows use under a wide range of microscopes. We further optimized the cell design for easy assembly. Dedicated sample holders for side-by-side and face-to-face arrangements of electrodes vastly improve the handling.
The ECC-Opto-10 is connected to the battery tester via 2 mm cell cable with banana plugs. It can be used with the PAT-Tester-x-8 as well as potentiostats and battery testers from third-party manufacturers.

Features

High cycling stability due to improved sealing concept

Dedicated sample holders for different electrode arrangements available

Fast assembly and dismantling and easy cleaning of cell components

Electrodes are easily accessible for post-mortem analysis

Low cell height of 21.5 mm for trouble-free use under many light microscopes

Fits well on standard microscope sample stages (76 × 26 mm (DIN ISO 8037-1))

Manual


	ECC-Opto-10 User Manual
	Release	1.27
	Date	September 2024
	Type	PDF
	Size	1.8 MB
Download

Specifications


Height	21.5 mm
Width	51 mm (base), 55 mm (in total)
Depth	75 mm (base), 77.5 mm (in total)
Weight	0.3 kg
Electrode dimensions	up to 10 mm
Operational temperature range	-20° to +70°C
Dead volume	1.8 cm³

Delivery scope

Item name	Order no.
ECC-Opto-10 test cell
Window seal (10 pcs.)	ECC1-05-0016-B/X
PE Sealing foil (10 pcs.)	ECC1-05-0032-A/X
Separator 10.0 mm x 0.26 mm, GF/A (10 pcs.)	ECC1-01-0012-R/X
Torque screwdriver, 0.2 Nm, cross handle	WZG9021
Inbus bit 1.5 mm x 1/4 inch	WZG9046
Hexagon screwdriver 2.5 mm, cross handle	WZG9047
Loading tweezer	ECC1-09-2010-B
Contact ring (face to face)	ECC1-05-0039-C
Contact disc 1.4404 (100x)	ECC1-05-0042-A
Contact disc 1.4404 (200x)	ECC1-05-0042-B
Contact disc 1.4404 (50x)	ECC1-05-0042-C
Sample holder side-by-side	ECC1-05-0040-B

Consumables

Item name	Order no.	Order
Separator 10.0 mm x 0.26 mm, GF/A, 50 pcs	ECC1-01-0012-R/L	Buy online
PE Sealing foil, 10 pcs	ECC1-05-0032-A/X	Buy online
Window seal, 10 pcs	ECC1-05-0016-B/X	Buy online

Spare parts

Test cell

Lid assembly

A newly developed sealing concept utilizing laser-welded glass-to-metal electrode feedthroughs and foil seals substantially increases cycle stability compared to the previous generation. The much more compact and low profile design allows use under a wide range of microscopes. We further optimized the cell design for easy assembly. Dedicated sample holders for side-by-side and face-to-face arrangements of electrodes vastly improve the handling.

The ECC-Opto-10 is connected to the battery tester via 2 mm cell cable with banana plugs. It can be used with the PAT-Tester-x-8 as well as potentiostats and battery testers from third-party manufacturers.

ECC-Opto-Std overview

Features

High cycling stability due to improved sealing concept

Dedicated sample holders for side-by-side and face-to-face electrode arrangements available

Fast assembly and dismantling and easy cleaning of cell components

Electrodes are easily accessible for post-mortem analysis

Low cell height of 21.5 mm for trouble-free use under many light microscopes

Fits well on standard microscope sample stages (76 × 26 mm (DIN ISO 8037-1))

Specifications


Height	21.5 mm
Width	51 mm (base), 55 mm (in total)
Depth	75 mm (base), 77.5 mm (in total)
Weight	0.3 kg
Electrode dimensions	up to 10 mm
Operational temperature range	-20° to +70°C
Dead volume	1.8 cm³

Manual


	ECC-Opto-10 User Manual
	Release	1.27
	Date	September 2024
	Type	PDF
	Size	1.8 MB
Download

Delivery scope

Item name	Order no.
ECC-Opto-10 test cell
Window seal (10 pcs.)	ECC1-05-0016-B/X
PE Sealing foil (10 pcs.)	ECC1-05-0032-A/X
Separator 10.0 mm x 0.26 mm, GF/A (10 pcs.)	ECC1-01-0012-R/X
Torque screwdriver, 0.2 Nm, cross handle	WZG9021
Inbus bit 1.5 mm x 1/4 inch	WZG9046
Hexagon screwdriver 2.5 mm, cross handle	WZG9047
Loading tweezer	ECC1-09-2010-B
Contact ring (face to face)	ECC1-05-0039-C
Contact disc 1.4404 (100x)	ECC1-05-0042-A
Contact disc 1.4404 (200x)	ECC1-05-0042-B
Contact disc 1.4404 (50x)	ECC1-05-0042-C
Sample holder side-by-side	ECC1-05-0040-B

Consumables

Item name	Order no.	Order
Separator 10.0 mm x 0.26 mm, GF/A, 50 pcs	ECC1-01-0012-R/L	Buy online
PE Sealing foil, 10 pcs	ECC1-05-0032-A/X	Buy online
Window seal, 10 pcs	ECC1-05-0016-B/X	Buy online

Spare parts

Test cell

Lid assembly

Accessories

Lid unit (OPTO-10) 18 mm Sapphire (22×0.3 mm)

Item name	Data
Lid opening	18 mm
Supported window size	22 x 0.3 +/- 0.1 mm
Content	preassembled lid unit with sapphire window
Order no.	ECC1-05-0010-B
Purpose	Suitable for stable window materials such as sapphire glass

Lid unit (OPTO-10) 10 mm Borosilicate (22×0.3 mm)

Item name	Data
Lid opening	10 mm
Supported window size	22 x 0.3 +/- 0.1 mm
Content	preassembled lid unit with borosilicate window
Order no.	ECC1-05-0010-C
Purpose	Suitable for less stable window materials like borosilicate

Lid unit (OPTO-10) 10×12 mm Beryllium (22×0.2 mm), theta > 5°

Item name	Data
Lid opening	10 x 12 mm
Supported window size	22 x 0.2 +/- 0.1 mm
Content	preassembled lid unit with beryllium window
Order no.	ECC1-05-0010-H
Note	theta > 5°, Inspection area (theta > 5°) = 1 mm

Lid unit (OPTO-10) 18 mm (22×0.25 mm with slit mask)

Item name	Data
Lid opening	18 mm
Supported window size	22 x 0.25 +/- 0.1 mm
Content	lid unit without window
Order no.	ECC1-05-0010-G
Note	Suitable for unstable window materials such as PET. The opening size and shape of the slit mask can be changed upon customer request.

Dedicated sample holders

Improve your workflow and save time with our sample holders for side-by-side and face-to face arrangements of electrodes. Both variants are included with each PAT-Cell-Opto-10 or ECC-Opto-10!

Sample holder (side-by-side)

Cycling of graphite vs Li in a side-by-side arrangement

Sample holder (face-to-face)

Contact discs with 1, 2, and 4 mm opening are available and included with each test cell.

Cycling of graphite vs Li in face-to-face arrangement

Video

Assembly procedures for side-by-side electrode setup (07/2022)

In this updated video, Dr. Matthias Hahn shows the required steps for assembling the test cell in the side-by-side electrode setup inside the glove box.

Item name	Resolution	Date	Type	Size
EL-CELL ECC-Opto-10 Assembly with Side-by-Side Sample Holder (07/2022)	1920x1080px	07/2022	mov	231 MB	Download

Assembly procedures for face-to-face electrode setup (10/2021)

Learn how to assemble the ECC-Opto-10 optical battery test cell in face-to-face electrode setup.

Item name	Resolution	Date	Type	Size
ECC-Opto-10: Assembly procedures for face-to-face electrode setup (10/2021)	1920x1080px	10/2021	mov	270 MB	Download

Sample test results

The picture shows two lithium metal electrodes – 20 µm lithium foil laminated on copper foil – beneath the sapphire window of the test cell. The electrodes are embedded into a glass fiber separator soaked with electrolyte. Applying a current of 20 µA for 5 hours makes the lithium to dissolve from the supporting copper foil (right electrode) and to plate as dendrites on the opposite side (left electrode).

The picture shows two graphite electrodes embedded in a glass fiber separator soaked with electrolyte. The graphite electrode on the left is being lithiated from the lithium metal electrode below the separator. From the color change, one can infer the lithiation gradient within the graphite electrode. The right graphite electrode can be used in a follow-up experiment to send lithium ions back and forth between the two graphite strips.