ECC-Opto-Std-Aqu

ECC-Opto-Std-Aqu

Test cell for optical characterization in the reflective mode with face-to-face arrangement of electrodes. For aqueous electrochemistry.

ECC-Opto-Std-Aqu

Test cell for optical characterization in the reflective mode with face-to-face arrangement of electrodes. For aqueous electrochemistry.

ECC-Opto-Std-Aqu

Test cell for optical characterization in the reflective mode with face-to-face arrangement of electrodes. For aqueous electrochemistry.

Product overview

Product description

The ECC-Opto-Std-Aqu test cell serves to monitor the optical properties of an electrode material in the course of electrochemical charging. For this purpose, the working electrode (WE) material, which is supported on a meshed or holed current collector, is placed right below the optical window. This WE is sandwiched from below with a glass fiber separator and an appropriate counter electrode (CE).

This way, the optical instrument “looks” from the top through the optical window onto the backside of the electrode material. Typical instrumentations include optical and confocal Raman microscopy in the reflection mode. Special window materials such as saphire, beryllium, polyimide are available. Please refer to the separate manual of the ECC-Opto-Std.

Features

2- and 3-electrode cell with optical window for aqueous electrochemistry

Materials in media contact are gold, PEEK and EPDM

The backside of the working electrode material can be observed through the optical window on top. Inspection area diameter is 1 mm. Other diameters up to 10 mm available.

Typically used in combination with optical or Raman microscopy in the reflection mode.

Working electrodes can be single crystals or grains, powder samples and free-standing electrodes (applied onto current collector mesh). Maximum electrode diameter is 10 mm.

Easy and clean electrolyte filling via the vacuum (syringe) method.

Specifications

Height46 mm
Width88 mm
Depth64 mm
Weightapprox. 0.2 kg
Electrode diameter10 mm
Electrolyte volumemin. 0.1 ml
Temperature operation range-20°C to +70°C

Manual

ECC-Opto-Std-Aqu User Manual
Release1.2
TypePDF
Size2.0 MB
Download

Delivery scope

ComponentOrder no.
ECC-Opto-Std-Aqu test cell with stand
ECC-Opto cell cableECE1-00-0075-A
Accessories kit:
Glass windows (5 pcs.)LAB0018/V
Glass fiber separators (5 pcs.) ECC1-01-0012-J/V
Feed wire, assy (Au)ECC1-00-0010-O
Holed current collector Au (5 pcs.)ECC1-00-0123-G/V
Filling tube with syringe (5 ml) for vacuum fillingECC1-01-0001-A
O-Ring 6.75 mm x 1.78 mmDIC9013
O-Ring 16 mm x 1.8 mmDIC9012
Hex wrench 0.9 mmWZG9005
Spherical hex screw driver 3 mmWZG9002

Spare parts

Test cell

Central CE Piston

REF electrode Opto (Au)

Electrode feed wire, Opto (Au)

Product overview

Product description

The ECC-Opto-Std-Aqu test cell serves to monitor the optical properties of an electrode material in the course of electrochemical charging. For this purpose, the working electrode (WE) material, which is supported on a meshed or holed current collector, is placed right below the optical window. This WE is sandwiched from below with a glass fiber separator and an appropriate counter electrode (CE).

This way, the optical instrument “looks” from the top through the optical window onto the backside of the electrode material. Typical instrumentations include optical and confocal Raman microscopy in the reflection mode. Special window materials such as saphire, beryllium, polyimide are available. Please refer to the separate manual of the ECC-Opto-Std.

Features

2- and 3-electrode cell with optical window for aqueous electrochemistry

Materials in media contact are gold, PEEK and EPDM

The backside of the working electrode material can be observed through the optical window on top. Inspection area diameter is 1 mm. Other diameters up to 10 mm available.

Typically used in combination with optical or Raman microscopy in the reflection mode.

Working electrodes can be single crystals or grains, powder samples and free-standing electrodes (applied onto current collector mesh). Maximum electrode diameter is 10 mm.

Easy and clean electrolyte filling via the vacuum (syringe) method.

Specifications

Height46 mm
Width88 mm
Depth64 mm
Weightapprox. 0.2 kg
Electrode diameter10 mm
Electrolyte volumemin. 0.1 ml
Temperature operation range-20°C to +70°C

Manual

ECC-Opto-Std-Aqu User Manual
Release1.2
TypePDF
Size2.0 MB
Download

Delivery scope

ComponentOrder no.
ECC-Opto-Std-Aqu test cell with stand
ECC-Opto cell cableECE1-00-0075-A
Accessories kit:
Glass windows (5 pcs.)LAB0018/V
Glass fiber separators (5 pcs.) ECC1-01-0012-J/V
Feed wire, assy (Au)ECC1-00-0010-O
Holed current collector Au (5 pcs.)ECC1-00-0123-G/V
Filling tube with syringe (5 ml) for vacuum fillingECC1-01-0001-A
O-Ring 6.75 mm x 1.78 mmDIC9013
O-Ring 16 mm x 1.8 mmDIC9012
Hex wrench 0.9 mmWZG9005
Spherical hex screw driver 3 mmWZG9002

Spare parts

Test cell

Central CE Piston

REF electrode Opto (Au)

Electrode feed wire, Opto (Au)

The ECC-Opto-Std-Aqu test cell serves to monitor the optical properties of an electrode material in the course of electrochemical charging. For this purpose, the working electrode (WE) material, which is supported on a meshed or holed current collector, is placed right below the optical window. This WE is sandwiched from below with a glass fiber separator and an appropriate counter electrode (CE).

This way, the optical instrument “looks” from the top through the optical window onto the backside of the electrode material. Typical instrumentations include optical and confocal Raman microscopy in the reflection mode. Special window materials such as saphire, beryllium, polyimide are available. Please refer to the separate manual of the ECC-Opto-Std.

ECC-Opto-Std-Aqu overview

Features

Features

2- and 3-electrode cell with optical window for aqueous electrochemistry

Materials in media contact are gold, PEEK and EPDM

The backside of the working electrode material can be observed through the optical window on top. Inspection area diameter is 1 mm. Other diameters up to 10 mm available.

Typically used in combination with optical or Raman microscopy in the reflection mode.

Working electrodes can be single crystals or grains, powder samples and free-standing electrodes (applied onto current collector mesh). Maximum electrode diameter is 10 mm.

Easy and clean electrolyte filling via the vacuum (syringe) method.

Specifications

Specifications

Height46 mm
Width88 mm
Depth64 mm
Weightapprox. 0.2 kg
Electrode diameter10 mm
Electrolyte volumemin. 0.1 ml
Temperature operation range-20°C to +70°C
Manual

Manual

ECC-Opto-Std-Aqu User Manual
Release1.2
TypePDF
Size2.0 MB
Download
Delivery scope

Delivery scope

ComponentOrder no.
ECC-Opto-Std-Aqu test cell with stand
ECC-Opto cell cableECE1-00-0075-A
Accessories kit:
Glass windows (5 pcs.)LAB0018/V
Glass fiber separators (5 pcs.) ECC1-01-0012-J/V
Feed wire, assy (Au)ECC1-00-0010-O
Holed current collector Au (5 pcs.)ECC1-00-0123-G/V
Filling tube with syringe (5 ml) for vacuum fillingECC1-01-0001-A
O-Ring 6.75 mm x 1.78 mmDIC9013
O-Ring 16 mm x 1.8 mmDIC9012
Hex wrench 0.9 mmWZG9005
Spherical hex screw driver 3 mmWZG9002
Spare parts

Spare parts

Test cell

Central CE Piston

REF electrode Opto (Au)

Electrode feed wire, Opto (Au)

Accessories

Optional window kits

As a standard, the ECC-Opto-Std-Aqu is equipped with a borosilicate glass window. Depending on your testing purposes the following additional window kits are available. Each kit includes one or more windows and a modified cell lid.

Always check compatibility (corrosion resistance, solubilitity) of the window material under the experimental conditions applied.

ECC-Opto Beryllium window kitECC1-00-0156-B
Purpose:X-Ray characterization
Content:
Beryllium window (1 pc)ECC1-00-0222-A
Lid (1 pc)ECC1-00-0127-C
Min. viewing angle: ≥8°


ECC-Opto Polyimide window kitECC1-00-0156-F
Purpose:X-Ray characterization
Content:
Polyimide (Cirlex) window (3 pcs)ECC1-00-0250-A
Lid (1 pc)ECC1-00-0127-C


ECC-Opto Zinc selenide window kitECC1-00-0156-D
Purpose:IR characterization
Content:
Zinc selenide window (1 pc)ECC1-00-0250-B
Lid (1 pc)ECC1-00-0127-E
Zinc selenide reacts with lithium metal or lithiated graphite. It is not recommended to be used in this combination.


ECC-Opto Calcium fluoride window kitECC1-00-0156-E
Purpose:IR characterization
Content:
Calcium fluoride window (1 pc)ECC1-00-0250-C
Lid (1 pc)ECC1-00-0127-E


ECC-Opto Sapphire window kitECC1-00-0156-C
Purpose:Raman characterization and light microscopy
Content:
Sapphire window (1 pc)ECC1-00-0149-A
Lid (1 pc)ECC1-00-0127-B

Cell holder I for ECC-Opto-Std

The Cell holder I is designed for the use of the ECC-Opto-Std in light microscopes.  It fits nicely on sample stages of most manufacturers (e.g. Thermofisher or Renishaw) utilizing standard microscope slides (75 x 26 mm, ISO 8037-1).

Specifications

Height32 mm
Width75 mm
Depth50 mm
Weight142 g

Cell holder II for ECC-Opto-Std

The Cell holder II is designed for the use of the ECC-Opto-Std in XRD microscopes like the Bruker D8.

Specifications

Height41,3 mm
Width78 mm
Depth76 mm
ECC-Opto-Std mounted on a Cell holder II

Cell holder III for ECC-Opto-Std

The Cell holder III is designed for the use of the ECC-Opto-Std in a Bruker FTIR Hyperion 2000 microscope.

Specifications

Height20 mm
Width75 mm
Depth61,5 mm
Cell holder III for ECC-Opto-StdCell holder III for ECC-Opto-Std

The cell holders for our optical test cells can be customized for your specific needs. Just ask!

Accessories

Optional window kits

As a standard, the ECC-Opto-Std-Aqu is equipped with a borosilicate glass window. Depending on your testing purposes the following additional window kits are available. Each kit includes one or more windows and a modified cell lid.

Always check compatibility (corrosion resistance, solubilitity) of the window material under the experimental conditions applied.

ECC-Opto Beryllium window kitECC1-00-0156-B
Purpose:X-Ray characterization
Content:
Beryllium window (1 pc)ECC1-00-0222-A
Lid (1 pc)ECC1-00-0127-C
Min. viewing angle: ≥8°


ECC-Opto Polyimide window kitECC1-00-0156-F
Purpose:X-Ray characterization
Content:
Polyimide (Cirlex) window (3 pcs)ECC1-00-0250-A
Lid (1 pc)ECC1-00-0127-C


ECC-Opto Zinc selenide window kitECC1-00-0156-D
Purpose:IR characterization
Content:
Zinc selenide window (1 pc)ECC1-00-0250-B
Lid (1 pc)ECC1-00-0127-E
Zinc selenide reacts with lithium metal or lithiated graphite. It is not recommended to be used in this combination.


ECC-Opto Calcium fluoride window kitECC1-00-0156-E
Purpose:IR characterization
Content:
Calcium fluoride window (1 pc)ECC1-00-0250-C
Lid (1 pc)ECC1-00-0127-E


ECC-Opto Sapphire window kitECC1-00-0156-C
Purpose:Raman characterization and light microscopy
Content:
Sapphire window (1 pc)ECC1-00-0149-A
Lid (1 pc)ECC1-00-0127-B

Cell holder I for ECC-Opto-Std

The Cell holder I is designed for the use of the ECC-Opto-Std in light microscopes.  It fits nicely on sample stages of most manufacturers (e.g. Thermofisher or Renishaw) utilizing standard microscope slides (75 x 26 mm, ISO 8037-1).

Specifications

Height32 mm
Width75 mm
Depth50 mm
Weight142 g

Cell holder II for ECC-Opto-Std

The Cell holder II is designed for the use of the ECC-Opto-Std in XRD microscopes like the Bruker D8.

Specifications

Height41,3 mm
Width78 mm
Depth76 mm
ECC-Opto-Std mounted on a Cell holder II

Cell holder III for ECC-Opto-Std

The Cell holder III is designed for the use of the ECC-Opto-Std in a Bruker FTIR Hyperion 2000 microscope.

Specifications

Height20 mm
Width75 mm
Depth61,5 mm
Cell holder III for ECC-Opto-StdCell holder III for ECC-Opto-Std

The cell holders for our optical test cells can be customized for your specific needs. Just ask!

Accessories

Window kits

Optional window kits

As a standard, the ECC-Opto-Std is equipped with a borosilicate glass window. Depending on your testing purposes the following additional window kits are available. Each kit includes one or more windows and a modified cell lid. Further window materials like magnesium oxide, silicon dioxide,  silicon nitride or PET (Mylar®)­ are available on request.

 

ECC-Opto Beryllium window kitECC1-00-0156-B
Purpose:X-Ray characterization
Content:
Beryllium window (1 pc)ECC1-00-0222-A
Lid (1 pc)ECC1-00-0127-C
Min. viewing angle: ≥8°
ECC-Opto Polyimide window kitECC1-00-0156-F
Purpose:X-Ray characterization
Content:
Polyimide (Cirlex) window (3 pcs)ECC1-00-0250-A
Lid (1 pc)ECC1-00-0127-C
ECC-Opto Zinc selenide window kitECC1-00-0156-D
Purpose:IR characterization
Content:
Zinc selenide window (1 pc)ECC1-00-0250-B
Lid (1 pc)ECC1-00-0127-E
Zinc selenide reacts with lithium metal or lithiated graphite. It is not recommended to be used in this combination.
ECC-Opto Calcium fluoride window kitECC1-00-0156-E
Purpose:IR characterization
Content:
Calcium fluoride window (1 pc)ECC1-00-0250-C
Lid (1 pc)ECC1-00-0127-E
ECC-Opto Sapphire window kitECC1-00-0156-C
Purpose:Raman characterization and light microscopy
Content:
Sapphire window (1 pc)ECC1-00-0149-A
Lid (1 pc)ECC1-00-0127-B
Always check compatibility (corrosion resistance, solubilitity) of the window material under the experimental conditions applied.

Cell holder

Cell holder I for ECC-Opto-Std

The Cell holder I is designed for the use of the ECC-Opto-Std in light microscopes.  It fits nicely on sample stages of most manufacturers (e.g. Thermofisher or Renishaw) utilizing standard microscope slides (75 x 26 mm, ISO 8037-1).

Specifications

Height32 mm
Width75 mm
Depth50 mm
Weight142 g


Cell holder II for ECC-Opto-Std

The Cell holder II is designed for the use of the ECC-Opto-Std in XRD microscopes like the Bruker D8.

Specifications

Height41,3 mm
Width78 mm
Depth76 mm


Cell holder III for ECC-Opto-Std

The Cell holder III is designed for the use of the ECC-Opto-Std in a Bruker FTIR Hyperion 2000 microscope.

Specifications

Height20 mm
Width75 mm
Depth61,5 mm

Gallery

Recommended tools

ECC-RefLoad

Ref loading tool – Useful tool for conveniently loading the Ref-sleeve

Product details

EL-Cut

High Precision Cutting Tool eliminates torn and chipped electrode edges. The recommended size for use with the ECC-Opto-Std is 10 mm.

Product details

Related products

ECC-Opto-Std

Test cell for optical and X-ray characterization in the reflective mode with face-to-face arrangement of electrodes

Product details

ECC-Opto-SBS

Test cell for optical characterization in the reflective mode with side-by-side arrangement of electrodes

Product details

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