Data Sheet (PDF)

PAT-Tester-i-16:

ECD-4-nano

Battery Test Cell for Measuring the Electrode Expansion

Dilation Sensor Range:

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Documentation

0  μm

+ 125 μm

- 125  μm

PAT-Cell

Data Sheet (PDF)

PAT-Tester-i-16:

Measure the Half-Cell Expansion

ECD-4-nano

Battery Test Cell for Measuring the Electrode Expansion

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Documentation

Upper
Electrode

Lower
Electrode

Or Measure the Full Stack

Data Sheet (PDF)

PAT-Tester-i-16:

Additional Sensors:

-20 °C

ECD-4-nano

Battery Test Cell for Measuring the Electrode Expansion

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Documentation

+80 °C

Temperature Sensor

Pressure Sensor

3 bar

0

Electrochemical Dilatometer ECD-4-nano

Advanced test cell for measuring the expansion and contraction of the electrodes in the nanometer range.

Typical Use Cases


  • Measuring the Expansion of a Single Electrode (3‑electrode Setup)

  • Measuring the Expansion of the Full Cell Stack (2‑electrode Setup)

  • Electrochemical testing with aprotic electrolytes

Key Features

Capacitive displacement sensor (range 250 μm, resolution ≤ 5 nm)

Additional gas pressure (0 to 3 bar) and temperature sensor (-20 to 80° C)

Cableless cell connection for easy handling and low setup time

Adjustable force on electrode/cell stack (up to 20 N/cm²)

PAT-Button for automatic cell identification in EL-Software

Sample Test Results

Measuring the thickness change of the graphite electrode (ECD-4-nano in single electrode operation mode)

Product Description

The ECD‑4‑nano is a high‑resolution electrochemical dilatometer for quantifying thickness changes with a resolution of better than 5 nanometers. It can measure either the thickness change of the individual electrode or that of the cell stack consisting of anode and cathode. Its capacitive parallel plate sensor offers exceptional stability and sensitivity while the force applied to the electrode can be continuously adjusted between 1 and 15 N (up to 20 N/cm²). This means that even single-sided coated and heavily calendered electrodes, which can bend significantly during charging, can be measured.

Additional sensors for gas pressure and temperature are installed as standard, supplementing the options for sample characterization.

The test cell features a corrosion‑resistant base and offers superior tightness against ambient athmosphere, enabling stable long‑term operation and compatibility with a wide range of electrolytes. The ECD‑4‑nano is connected cablelessly to the PAT socket of a PAT-tester-x-8 or PAT‑Stand‑1 to minimize cable‑induced artifacts and simplify handling and installation. The integrated PAT-Button enables automatic cell detection in EL-Software.

Product Update 2025: What’s new?

New features:

  • Adjustable Force 1-15 N

Improvements:

  • Adjustment of the sensor head. New optional ECD-4 Centering Device for direct visual feedback (when using a PAT-Tester-x-8 as potentiostat)
  • Rotation Lock for Allen wrench
  • Frit Flange (improved protection against electrolyte spillage, improved height adjustment, reinforcement against deformation)
  • Adjusted spacer disc diameter

Working Modes

Half-Cell Mode with reference electrode

A stiff glass frit, soaked in electrolyte, separates the working electrode (WE) from the counter electrode (CE). The upper WE is sealed using a flexible metal membrane, through which any charge-induced thickness change is transmitted toward the sensor/load unit attached on top. The glass frit’s fixation ensures that only the thickness change of the working electrode is detected without interference from the CE.

Full-Cell Mode (2-electrode measurement)

Both electrodes are separated by a thin (a few 10 microns) separator. The cell stack is sealed at the top by a flexible metal membrane through which any charge-induced change in thickness is transmitted toward the sensor/load unit mounted above. The lower electrode rests on a stainless steel current collector. In this setup, the thickness change of the entire cell stack is recorded.

The optional ECD-4 Full Cell Kit is required for this setup. See the accessories section for morge details.

Specifications

Length 77 mm
Width 68 mm
Height with/without attached sensor cable 272 / 173 mm
Weight 2 kg
Electrode diameter max. 10 mm
Electrode thickness Half cell mode: max. 1 mm
Full cell mode: max. 1 mm (combined value for electrodes and separator)
Glass T-Frit (Separator) Diameter 12.5 mm / 10 mm Thickness 3.5 mm
Separator diameter (full cell mode) max. 10 mm
Cell electrolyte volume approx. 240 μl with T-frit (half cell mode)
approx. 40 μl in full cell mode approx.. 40 μl in full cell mode
Gas pressure sensor: 0 to 3 bar abs.
Temperature sensor -20 to 80° C
Chemical compatibility Aprotic organic electrolytes
Cell electrolyte volume Half cell mode: approx. 0.2 ml Full cell mode: approx. 0.03 ml
Operational temperature range (cell and sensor) -20 to 80° C
Operational temperature range (conditioning electronics and data logger) 0 to 40 °C
Load on test specimen approx. 1 to 15 Newton
Displacement sensor type: Capacitive
Displacement range: 250 μm
Displacement resolution: ≤ 5 nm
WordPress Data Table

Documentation

WordPress Data Table

Battery Test Cell for Measuring Gas Evolution / Consumption

The ECD‑4‑nano is a high‑resolution electrochemical dilatometer for quantifying thickness changes with a resolution of better than 5 nanometers. It can measure either the thickness change of the individual electrode or that of the cell stack consisting of anode and cathode. Its capacitive parallel plate sensor offers exceptional stability and sensitivity while the force applied to the electrode can be continuously adjusted between 1 and 15 N (up to 20 N/cm²). This means that even single-sided coated and heavily calendered electrodes, which can bend significantly during charging, can be measured.

Additional sensors for gas pressure and temperature are installed as standard, supplementing the options for sample characterization.

The test cell features a corrosion‑resistant base and offers superior tightness against ambient athmosphere, enabling stable long‑term operation and compatibility with a wide range of electrolytes. The ECD‑4‑nano is connected cablelessly to the PAT socket of a PAT-tester-x-8 or PAT‑Stand‑1 to minimize cable‑induced artifacts and simplify handling and installation. The integrated PAT-Button enables automatic cell detection in EL-Software.

ECD-4-nano Overview

Typical Use Cases

  • Measuring the Expansion of a Single Electrode (3‑electrode Setup)
  • Measuring the Expansion of the Full Cell Stack (2‑electrode Setup)
  • Electrochemical testing with aprotic electrolytes

Features

Capacitive displacement sensor (range 250 μm, resolution ≤ 5 nm)

Additional gas pressure (0 to 3 bar) and temperature sensor (-20 to 80° C)

Cableless cell connection for easy handling and low setup time

Adjustable force on electrode/cell stack (1 to 15 N)

PAT-Button for automatic cell identification in EL-Software

Specifications
Length 77 mm
Width 68 mm
Height with/without attached sensor cable 272 / 173 mm
Weight 2 kg
Electrode diameter max. 10 mm
Electrode thickness Half cell mode: max. 1 mm
Full cell mode: max. 1 mm (combined value for electrodes and separator)
Glass T-Frit (Separator) Diameter 12.5 mm / 10 mm Thickness 3.5 mm
Separator diameter (full cell mode) max. 10 mm
Cell electrolyte volume approx. 240 μl with T-frit (half cell mode)
approx. 40 μl in full cell mode approx.. 40 μl in full cell mode
Gas pressure sensor: 0 to 3 bar abs.
Temperature sensor -20 to 80° C
Chemical compatibility Aprotic organic electrolytes
Cell electrolyte volume Half cell mode: approx. 0.2 ml Full cell mode: approx. 0.03 ml
Operational temperature range (cell and sensor) -20 to 80° C
Operational temperature range (conditioning electronics and data logger) 0 to 40 °C
Load on test specimen approx. 1 to 15 Newton
Displacement sensor type: Capacitive
Displacement range: 250 μm
Displacement resolution: ≤ 5 nm
WordPress Data Table

Recommended Potentiostats/PAT docking stations

Documentation
ECD-4-nano User Manual
Release 1.42
Date February 2025
Type PDF
Size 3 MB
Download
PAT-Cell Data Sheet
Date November 2025
Type PDF
Size 0.5 MB
Download
WordPress Data Table
Consumables
Name Order No. Order
PE Sealing, 10 pcs. ECC1-06-0043-A/X Buy online
T-Frit 10 mm/12.5 mm/3.5 mm, 10 pcs. ECC1-06-0041-A/X Buy online
Reference Ring II, Li coated, ECD-4-nano, 10 pcs. ECC1-01-0078-B/X Buy online
Accessories

ECD-4 full cell kit (Order no.: ECC1-00-0379-A )

This optional set contains all parts needed for measuring the expansion of full cell stack in the ECD-4-nano.

Cell assembly block III (Order no.: ECC1-02-0045-A )


The Cell Assembly Block enables safe working with torque wrenches without the test cell slipping away. It fits all battery test cells in the PAT series.

 

 

 

ECD-4 Centering Device (Order no.: ECE1-00-0400-A)

The ECD-4 Centering Device is an optional accessory that can be mounted on the PAT-Stand-1 docking station. It provides direct visual feedback on the set sensor position. To use this device, you must connect the PAT-Stand-1 to a PAT-tester-x-8 potentiostat. The Centering device can remain permanently connected to the PAT-Stand-1.

Spare parts

ECD-4-nano

 

Cell base

 

Screw Cap Unit

 

Frit Flange Unit

 

Sensor Cable

Sample Test Results

Measuring the thickness change of the graphite electrode (ECD-4-nano in single electrode operation mode)

Accessories, Consumables & Spare Parts

ECD-4 full cell kit (Order no.: ECC1-00-0379-A )

This optional set contains all parts needed for measuring the expansion of full cell stack in the ECD-4-nano.

Cell assembly block III (Order no.: ECC1-02-0045-A )


The Cell Assembly Block enables safe working with torque wrenches without the test cell slipping away. It fits all battery test cells in the PAT series.

ECD-4 Centering Device (Order no.: ECE1-00-0400-A)

The ECD-4 Centering Device is an optional accessory that can be mounted on the PAT-Stand-1 docking station. It provides direct visual feedback on the set sensor position. To use this device, you must connect the PAT-Stand-1 to a PAT-tester-x-8 potentiostat. The Centering device can remain permanently connected to the PAT-Stand-1.

Name Order No. Order
PE Sealing, 10 pcs. ECC1-06-0043-A/X Buy online
T-Frit 10 mm/12.5 mm/3.5 mm, 10 pcs. ECC1-06-0041-A/X Buy online
Reference Ring II, Li coated, ECD-4-nano, 10 pcs. ECC1-01-0078-B/X Buy online

ECD-4-nano

 

Cell base

 

Screw Cap Unit

 

Frit Flange Unit

 

Sensor Cable

Recommended tools

EL-Cut

High precision cutting pliers to eliminate torn and chipped electrode edges. Recommended diameter size for use with the ECD-4-nano is 10 mm.

Product details

ECC-LiPunch

Punching tool for lithium foil. The recommended size for use with the ECD-4-nano is 10 mm.

Product details

Related products

EL-CELL PAT-Tester-x-8

PAT-Tester-x-8

Modular multi-channel potentiostat for special and small-scale testing
Product details

PAT Stand-1

The ideal docking station for individual battery testing

Product details

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